- How long does certification
last?
ANSWER: All certified and applied laboratories
are required to annually renew their certification.
The certification year runs concurrent to the state's
fiscal year of July 1 through June 30.
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- Once I apply for
certification, how long will it take me to become
certified?
ANSWER: All applications are given the highest
priority for review (typically within two weeks)
by the Programs Technical staff. Each Application
Package is checked for completeness of Part I-Administrative
Information, Part II-Personnel and Part III-Analytical
Testing Parameters. Upon receipt of the application,
the OQA will advise the applicant in writing whether
the application is administratively complete and
will assign the laboratory a five-digit identification
number. A determination that the application is
administratively complete does not authorize the
laboratory to perform sample handling, preservation,
and analyses and reporting of data as regulated
by N.J.A.C. 7:18. Once the application has been
determined administratively complete, the laboratory
will be contacted by a Laboratory Certification
Officer (LCO). That LCO will request the submittal
of additional information and schedule an on-site
audit of the laboratory. Upon submittal of all required
information and acceptable responses to any deficiencies
noted in applicable documentation or that were identified
in an on-site audit, the laboratory will be granted
certification through issuance of a certificate
and an Annual Certified Parameters List noting Certified
status in the applicable analytical methods. This
process can be completed in as little as 45 days.
Extended time periods occur when deficiencies are
noted during the application process or during the
on-site audit.
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- Does my facility need
to be certified to sample and measure pH for the
PWTA?
ANSWER: Yes. pH analysis for the PWTA must
be performed by a facility certified to perform
pH. Sampling for pH for the PWTA must be performed
by an employee or authorized representative of a
certified laboratory. However, since the holding
time for a pH sample is 15 minutes, it is likely
that the sampling will need to be performed by a
laboratory certified for pH.
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- How do I get approval
for a test method that is different than that
certified by the NJDEP, OQA?
ANSWER: Laboratories requesting certification
for a test method not included on the list of DSAMs
offered by the Department should contact the OQA.
The OQA may approve the use of alternate test methods
under the authority of N.J.A.C. 7:18. Please contact
the OQA at 609-292-3950 for details.
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- Is there a reduced fee
for secondary NELAC certification?
ANSWER: There is no reduced fee for secondary
NELAC certification.
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- Do I need to complete
the entire Part II when I renew certification?
ANSWER: Part II must always be submitted
with a renewal application. However, it needs only
to be completed in its entirety if laboratory personnel
have changed since the application was last completed.
Specific instructions for completing Part II can
be found on the "Laboratory Certification Programs"
page of this site.
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- Do analyze immediately
parameters need to be performed by a certified
laboratory?
ANSWER: Yes, testing for all parameters including
analyze immediately parameters such as temperature
and pH, must be performed by a laboratory certified
to perform those measurements.
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- Why should my laboratory
seek NELAP certification as opposed to ELCP certification?
ANSWER: This is a choice to be made by each
lab. For a laboratory that is certified in several
states, NELAP certification may reduce the number
of audits a laboratory would need to receive, thereby
reducing costs. Information on the NELAP program
can be obtained at www.nelac-institute.org.
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- As a certified laboratory,
what do I need to do to obtain certification for
an additional parameter or method?
ANSWER: A laboratory seeking additional certifications
shall submit a modified application, including Parts
I, II and III to the OQA. Application forms can
be found on "Laboratory Certification Programs"
page of this site.
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- Do certified laboratories
have to maintain certification for the verification
step for total coliform in support of the total
coliform rule?
ANSWER: Yes. N.J.A.C. 7:18-4.1(b) requires
that a laboratory qualifying for certification to
perform total coliform testing on samples for compliance
with the Bureau of Safe Drinking Water's program
must concurrently qualify to perform fecal coliform
and/or E.Coli. testing so that the presence/absence
of either can be detected and reported within the
specified time limits.
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- How can I find out what
laboratories are certified for the analysis of
a particluar pollutant in drinking water, wastewater,
solid-hazardous waste, or air?
ANSWER: A list of laboratories can be found
on the "Find a Certified Lab" link on
this website or by contacting the OQA at (609)292-3950.
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- How can I get my drinking
water tested? Can it be done for free?
ANSWER: The NJDEP does not provide free drinking
water testing. Costs for drinking water tests are
paid by the property owner. A list of laboratories
that are certified to perform drinking water testing
can be found on the "Find a Certified Lab"
link on this website or by contacting the OQA at
(609)292-3950.
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- To gain initial certification,
is a laboratory required to use PT’s through
the NJ program?
ANSWER: For initial certification a PT sample
may be obtained from any NIST approved provider.
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- Who are the OQA-approved
PT providers?
ANSWER: The NJ approved PT providers are
Analytical Products Group (APG), Environmental Resource
associates (ERA), SPEX Certiprep, Protocol, and
Microcheck.
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- When are the PT studies
scheduled for?
ANSWER: The Drinking Water studies are conducted
in January and July. The Waste Water studies are
conducted in June and December. The Solid/Hazardous
Waste studies are conducted in October and April.
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- Can I use the NJ DEP
Waste Water PT samples for my EPA DMRQA requirements?
ANSWER: For EPA Region 2 the NJ DEP Waste
Water PT samples will be accepted for the DMRQA
requirements. There may be an extra cost for this
from the PT provider to report the data. For other
EPA regions please contact your EPA coordinator.
The DMRQA results however may not be reported to
meet NJDEP wastewater requirements.
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- Are NELAP laboratories
required to do the PTs in NJ program that are
above and beyond the NELAC Fields of Testing to
maintain accreditation?
ANSWER: A NELAP laboratory will maintain
their accreditation for these parameters without
doing the PT samples. However, in order to report
data to NJ for regulatory purposes, the laboratory
must analyze and pass one PT per year in NJ program
that are above and beyond the Fields of Testing.
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- What should I report
in the method code column?
ANSWER: When reporting NJ PT data the NJ
DEP parameter codes found on your Annual Certified
Parameter List (ACLP) are to be used as the Method
Codes.
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- Why did I fail my SDW
Microbiology samples if I passed either Total
or Fecal Coliform?
ANSWER: A laboratory must pass the SDW Microbiology
PT for both Total Coliform and Fecal Coliform or
E. Coli to perform Total Coliform analysis.
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- I don’t perform
analysis using a particular method, that I hold
certification for, do I have to analyze a PT?
ANSWER: You must analyze a PT for any method
where a PT is required if your are in applied or
certified status, regardless of whether testing
is currently being conducted using that method.
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- Will the OQA accept
PT data from other PT providers?
ANSWER: Petitions to use PT providers other
than those contained in the NJ DEP contract shall
be submitted, in writing, to the OQA. When approvals
are granted, the PT provider chosen must send the
PT results directly to the OQA.
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- What analytes/parameters
do I need to report PT data for?
ANSWER: You must report PT data for all parameters
in which you hold certification, that are listed
on the Analyte List/ Cost Table attached to the
PT letter.
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- Does NJ OQA want a
copy of my PT data?
ANSWER: No, copies of PT data are provided
directly to the Department by Department approved
PT providers, for those laboratories using the NJ
DEP approved PT providers. However, for those laboratories
using other providers, the laboratory must specifically
request that the PT provider submit results to the
Department.
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- When do I report my
PT data?
ANSWER: The reporting deadlines for each
PT study are specific to that study. Please reference
the reporting instructions sent with the PTs from
the PT provider. Note that if you are receiving
PTs from more then one provider, the PT due date
may be different for each provider.
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- I broke my PT/I received
my PT samples broken.
ANSWER: Complete the Sample Replacement Request
Form and fax it to (609) 777-1774 ASAP.
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- If my NJDEP-certified
laboratory is not performing regulatory analyses
for the NJDEP, must I use a certified laboratory?
ANSWER: If the analyses being performed are
for research or other non-regulatory purposes, the
New Jersey Laboratory Certification Regulations,
N.J.A.C., do not require the use of a certified
laboratory.
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- If I am using field
analytical methods such as immunoassay and XRF
for waste site characterization, must I be certified?
ANSWER: No as of July 2003, but the Department
expects to announce new initiatives for the remediation
of hazardous waste sites that will require any entity
performing field analytical measurements by; Immunoassay,
Field portable gas chromatography, Field portable
gas chromatography, or Field portable x-ray fluorescence
spectroscopy, to be certified for those methods.
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- Who should develop
a Qulity Assurance Program Plan (QAPP)?
ANSWER: Any person or group collecting samples
for the measurement of chemical and/or biological
parameters should develop a Quality Assurance Program
Plan (QAPP) prior to sampling. Staff of the OQA
can assist in developing and/or reviewing QAPPs.
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- Who has responsibility
to insure that QAPPs are carried out as approved?
ANSWER: The organization conducting the project.
The OQA can assist in helping to evaluate if the
QAPP is being followed.
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- What is a New Jersey
Quantitation Limit (NJQL)? How does the NJQL differ
from the Practical Quantitation Limit (PQL) or
other method limit terms?
ANSWER: The Department is proposing to adopt
NJQLs at N.J.A.C. 7:18-11. NJQLs are being created
to establish a level that can be achieved by the
current analytical capabilities of the New Jersey
certified laboratory community. The NJQL is defined
the lowest level of a substance that can be reliably
measured during routine laboratory operations. The
Department is proposing the use of NJQLs to assure
the reliability of measurements related to assessment
of water quality and compliance with applicable
regulatory requirements. It is intended that NJQLs
will be utilized as compliance levels when regulatory
requirements, such as NJPDES permit discharge limitations,
are not set at levels below what can accurately
and routinely quantified. NJQLs are calculated by
taking the Method Detection Limit, the lowest value
that can be distinguished from 0, and multiplying
that value by 5. The NJQL is the same concept as
the PQL, except the NJQL will be derived from data
only from NJDEP-certified analytical laboratories.
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- Can laboratories use
Freon 113 for Oil and Grease (O&G) and Total
Petroleum Hydrocarbon (TPH) analyses?
ANSWER: Yes, The laboratories may use recycled
Freon or Freon manufactured before December 31,
2001.
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- Is there a replacement
method for EPA 413.1 for O & G
ANSWER: Yes, EPA method 1664A N-Hexane Extractable
Material (HEM; Oil and Grease) is a replacement
for EPA method 413.1. Because the solvent is changed
from Freon to n-hexane the material extracted may
be different. The biggest differences are seen with
the analysis of animal and vegetable oil discharges.
A side by side comparison study should be done.
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- Is there a replacement
method for EPA 418.1 for TPH?
ANSWER: No, There is no direct replacement
for EPA method 418.1 THP. The 418.1 method extracts
a wide range of petroleum molecular weights (carbon
numbers), possibly C-8 to C-70. There are GC methods
using various solvents that can determine petroleum
hydrocarbons i.e. EPA SHW method 8015B DRO, (C-12
to C-28); NJ-DEP OQA-QAM-025 (C-8 to C-40).
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- Can EPA Method 1664
replace EPA Method 418.1?
ANSWER: No, Method 418.1 uses IR detection.
In method 1664A SGT-HEM the extract is heated at
85o C to remove the solvent before determining NMP.
Lower boiling THP are lost. The carbon range for
the method is not known.
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- Must wastewater samples
be distilled before measuring NH3 by ion-selective
electrode?
ANSWER: Yes, in 40 CFR 136 all the determinative
methods for ammonia are listed under ammonia distillation.
Therefore, the strict interpretation requires the
distillation of all wastewater samples. If a routine
sample can be shown to be free from interferences,
distillation is not required. The laboratory must
have side by side historical comparison data with
and without distillation to prove that interferences
are not present.
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- How do I obtain
copies of the analytical methods?
ANSWER: The internet has become an excellent
resource for official methods, including the US
EPA web pages. The most usable and complete example
is probably the National
Environmental Methods Index (NEMI), a joint
effort of EPA and USGS. This index is free and
searchable by source [for example Hach, or Standard
Methods], instrumentation, keyword such as analyte
name or CAS number or method number, and so forth.
It includes regulatory and non-regulatory analyses.
Searches typically yield lists, and then single-page
method summaries with hot links to sources.
Frequently a method is available as a .pdf file,
which can be downloaded or printed. Government sources
tend to be free, whereas there are generally fees
at some commercial sites.
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- Can I purchase
the dilution/rinse water for use in microbiological
testing?
ANSWER: N.J.A.C. 7:18-4.5(c)4 specifies analytical
requirements for rinse water. Many laboratories
purchase dilution/rinse water for use in microbiological
testing. Though this is acceptable, it is the responsibility
of the laboratory to ensure that the appropriate
testing is conducted on the water. If the testing
is not conducted by the manufacturer, it must be
conducted by the laboratory. As it is not standard
practice for all manufacturers to conduct this testing,
a laboratory should contact their provider to determine
whether the testing was conducted and that the company
supplying the water meets the requirements of the
rules. Specifically, the laboratory must request
assurance from the provider that:
- Only reagent grade water obtained from a still
or deionization unit is used as the "source
water" to make the dilution / rinse water
(phosphate buffer).
- Each batch or lot of the source water must be
tested for metals and bacteriological quality.
- The laboratory using the pre-purchased ready
to use dilution/rinse water is responsible for
testing monthly: heterotrophic bacteria, conductivity
and chlorine residual if the source water to the
still or deionization unit is chlorinated.
Records of the required analyses must be on file
at the laboratory for each batch or lot of dilution/rinse
water used, regardless of who conducted the testing.
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